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Paper
Grinding Discs
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In
order to obtain scrachfree surfaces without deformation, successive
material removal by abrasives is necessary. Grinding is the
next stage after sectioning. Grinding is divided into two
processes: Planar grinding and Fine grinding.
The purpose of planar grinding is to obtain a level surface
and to remove scale, burrs or surface irregulation from the
specimen. Coarse paper discs (up to 120 grit) are used for
planar grinding. Fine grinding removes the deformations resulting
from coarse grinding to make the surface ready for polishing
which is the final stage.
Metkon paper grinding discs are available as "Plain back"
(PL) and "Self Adhesive" (SA).
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Diamond
Grinding Pads
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Diamond
grinding pads are used especially for the leveling and grinding
of very hard materials such as ceramics, refractory materials
and tungsten carbides. Diamond pads have perfectly calibrated
diamond deposit coated by metallic or resinoid bands. Metal
bonds are used for planar grinding and resin bonds are good
for fine grinding.
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POLISHING
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To remove
deformation from fine grinding and obtain a surface that is
highly reflective, the specimens must be polished before they
can be examined under the microscope. Polishing is a complex
activity in which factors such as quality and suitability
for the cloth,abrasive, polishing pressure, polishing speed
and duration need to be taken into account. The quality of
the surface obtained after the final polishing depends on
all these factors and the finish of the surface on completion
of each of the previous stages.
Diamond
Products
Diamond,
due to its exceptional hardness and cutting capacity, has
become the first choice abrasive in metallographic polishing.
Diamonds for metallographic grinding and polishing are available
in two different crystalline shapes: Polycrystalline (P) and
monocrystalline (M). Polycrystalline diamonds provide vast
numbers of small cutting edges. In the metallographic preparation
process these edges result in high material removal, while
producing only a shallow scratch depth.
Monocrystalline diamonds are more block-shaped and provide
few cutting edges. These diamonds give high material removal
with a more variable scratch pattern. For high requirements,
the (P)-type diamond are chosen. The (M) type diamonds are
best suited for all-purpose polishing. METKON offers diamond
products in three forms; diamond paste, diamond suspension
and diamond spray.
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Diamond
Lubricant & Alumina
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Diamond
Lubricant, Water-based 1.0 lt., bottle
Alumina Suspensions
Alumina Powder (deaglomerated)
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Polishing
Cloths
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There are three types of polishing clothes; Woven, Non-Woven
and Flocked.
-Woven cloths offer 'hard surface' polishing properties and
guarantee flat pre-polishing, without deterioration of the edges.
-Non-woven cloths, are used on very hard materials for high
precision surface finishing such as glass, quartz, sapphire
and semi-conductors.
-The Flocked cloths, guarantee a super-polished finish. The
polishing duration must be as short as possible, to avoid inclusions
from being extracted. |
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MICROLOGUE®
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METKON MICROLOGUE® contains a number of case histories describing
various sample preparation methods and the results obtained
by applying these methods. It contains the conclusions of an
extensive and intense work that has been conducted at METKON
Application Lab.
If you are interested in any MICROLOGUE® Method, please
contact us through our website www.metkon.com.
We invite the input of our customers and colleagues in industry
and Academia regarding new and interesting sample preparation
challenges. For further information, please contact METKON Application
Lab.
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Material
: Nodular Cast Iron, Ferritic+ Pearlitic
Micrologue
Method No : B05
Results :
This type of cast iron has more toughness. Ferrite zones
( violet ) and perlite surround the nodular graphities.
Polarized light illumination is recommended to analyze
the graphites.
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| Preparation
Method : |
| Cutting
: METACUT cut-off machine with Ø250 TREN-S abrasive
wheel ( 19-023 ) |
| Mounting
: METAPRESS Mounting Press and DAP - Diallyphtalat Phenolic
Powder ( 29-012 ) |
| Mechanical
Preparation : GRIPO 1V Grinding / Polishing Machine
+ FORCIMAT Automatic Specimen Mover. |
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Parameter
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Stage
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Surface
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Abrasive
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Lubricant
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Force
per Sample, (N)
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Tim
min.
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Disc
Speed, rpm
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Relative
Rotation
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Planar
Grinding
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DEMPA
Paper Disc
38-040-240
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240
Grit
SIC
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Water
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25
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5
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120
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Contra
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MP
Step 1.
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DEMPA
Paper Disc
38-040-400
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400
Grit
SIC
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Water
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25
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5
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120
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Contra
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MP
Step 2.
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SATO-S Cloth
39-035-250
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Diam.6µ
DIAPAT
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DIALUB
39-502
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25
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5
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120
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Contra
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MP
Step 3.
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SATO-S
Cloth
39-035-250
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Diam.
1µ DIAPAT
39-311
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DIALUB
39-502
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25
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5
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120
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Comp.
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Final
Polishing
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FEDO-1N
Cloth
39-055-250
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ALU-M1K
0.05µ
Alum. Susp. 39-200
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Water
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15
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5
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120
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Comp.
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Etching
: %2Nital
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